Tough Old Man

Today I made my first test e. The directions I used was I added 10 grams of powder a beaker. then I added 1 ml of BA. Then 30 ml of sesame oil. I then place the beaker on a pan and heated while swirling it until it was clear looking. I then ran it through a filter. 1 hour has gone by and now I notice that it looks like it is separating or something. Looks like little white lines in it. Any ideas

Within a hr later it crysalized. I reheated it and it came back. 2 hrs. later it was worst then before. Today I throw out 3 40 ml vials. All were bad

PT

dg806

How much were you trying to make? At what mg/ml. What Ba %?
Your numbers only add up to 38.5
Were you making 50ml? If so we need to adjust some numbers.

"So as we set out this year to defeat the divisive forces that would take our freedom away, I want to say those words again for everyone within the sound of my voice to hear and to heed, and especially for you, Mr. Gore. From my cold dead hands!"




"I now begin the journey that will lead me into the sunset of my life. I know that for America there will always be a bright dawn ahead."
Nov. 5, 1994 - Ronald Reagan

Tough Old Man

I was making 40 ml. @ 250........10 grams of powder. 30 ml's of sesame oil. 1 ml BA

Here is the exact way I did it. I first heated the ool in a muffin pan. I took a beaker and added the powder, BA and oil all at once. Then I placed it on a skillet and heated it up until clear. Then ran it through a filter.. Left the vent needle in it until it cooled

Is it possible that I heated on a skillet to long and at to high of heat

dg806

You were using 2.5% BA @ 40ml. Ba IMO is more of a sterile agent. BB will help hold the powder in solution and not crash and will make it a little thinner and help with the pain( Less BA requied). Here is what I would do.

10g powder (.75 dispalcement x 10 = 7.5)
27.7 ml oil -
.8ml BA
4 ml BB

27.7+7.5+.8+4=40ml
Heat it gently...........not too hot or it will break down the gear.
This should hold no problem and be almost painless. I would run it through a .2 whatman. Baking should not really be necessary unless you want added protection.

"So as we set out this year to defeat the divisive forces that would take our freedom away, I want to say those words again for everyone within the sound of my voice to hear and to heed, and especially for you, Mr. Gore. From my cold dead hands!"




"I now begin the journey that will lead me into the sunset of my life. I know that for America there will always be a bright dawn ahead."
Nov. 5, 1994 - Ronald Reagan

Tough Old Man

Oh I get what you did. Have a question. When I put it into the calculator it say that for 40 ml's use 25.2 ml oil. That is with 10 g powder, 10% bb = 4 ml and 2% ba = .80. Why is the powder converter off. Well hell just used your calc that you have posted and see that it is 27.7.

dg806

Yeah the displacement of the powder is only 7.5ml
Use .75 for dry powder or .85 for wet powders(like eq)

"So as we set out this year to defeat the divisive forces that would take our freedom away, I want to say those words again for everyone within the sound of my voice to hear and to heed, and especially for you, Mr. Gore. From my cold dead hands!"




"I now begin the journey that will lead me into the sunset of my life. I know that for America there will always be a bright dawn ahead."
Nov. 5, 1994 - Ronald Reagan

MuscleM4n

Wow you make your own Test E!

That's soo cool

very clever guys we have here

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Tough Old Man

I have to disagree with you. It was the first time for me and I ended uo throwing out 3 40ml vials as it all went bad by the next day.