I do upper body on one day legs on the other.. M, Tues and T, Fri. I superset pulls and pushes if I'm short on time or for a change. One set pull.. one set push..and so on. I would not do pulls in one superset because my biceps are used set after set within the superset, not good. So here's an example.
Shoulder "press" and "pull" ups:
press a set
pull a set
press a set
rest
pull a set
press a set
rest
pull a set
press a set
rest
pull a set
rest
press a set
rest
pull set
I like reps of 6 and 60 sec or so rest time. Depending on the group of sets I may rest less or not at all.
It's best to alternate sets of opposite movements to do it right, IMHO. Or... different body parts can be used and it can be as many exercises as you want.
Example: neck curls, hams, wrist curls, calves and sit ups could make a good superset. So with that one it's 5 sets into one set....a superset, just like in math class.